PittsburghV1, Main, Exploration, bibRecord, 005373

In Situ Transmission Electron Microscopy Study of Electrochemical Sodiation and Potassiation of Carbon Nanofibers

Identifieur interne : 005373 ( Main/Exploration ); précédent : 005372; suivant : 005374

In Situ Transmission Electron Microscopy Study of Electrochemical Sodiation and Potassiation of Carbon Nanofibers

Auteurs : YING LIU [États-Unis] ; FEIFEI FAN [États-Unis] ; JIANGWEI WANG [États-Unis] ; YANG LIU [États-Unis] ; HAILONG CHEN [États-Unis] ; Katherine L. Jungjohann [États-Unis] ; YUNHUA XU [États-Unis] ; YUJIE ZHU [États-Unis] ; David Bigio [États-Unis] ; TING ZHU [États-Unis] ; CHUNSHENG WANG [États-Unis]

Source :

Nano letters : (Print) [ 1530-6984 ] ; 2014.

RBID : Pascal:14-0197204

Descripteurs français

Pascal (Inist)
- Microscopie électronique transmission, Carbone, Nanofibre, Nanomatériau, Bicouche, Sodium, Interface, Anisotropie, Réaction électrochimique, Microstructure, Electrode carbone, 8107V, 8107B, 6865.
Wicri :
- topic : Carbone, Sodium.

English descriptors

KwdEn :
- Anisotropy, Bilayers, Carbon, Carbon electrode, Electrochemical reaction, Interfaces, Microstructure, Nanofiber, Nanostructured materials, Sodium, Transmission electron microscopy.

Abstract

Carbonaceous materials have great potential for applications as anodes of alkali-metal ion batteries, such as Na-ion batteries and K-ion batteries (NIB and KIBs). We conduct an in situ study of the electrochemically driven sodiation and potassiation of individual carbon nanofibers (CNFs) by transmission electron microscopy (TEM). The CNFs are hollow and consist of a bilayer wall with an outer layer of disordered-carbon (d-C) enclosing an inner layer of crystalline-carbon (c-C). The d-C exhibits about three times volume expansion of the c-C after full sodiation or potassiation, thus suggesting a much higher storage capacity of Na or K ions in d-C than c-C. For the bilayer CNF-based electrode, a steady sodium capacity of 245 mAh/g is measured with a Coulombic efficiency approaching 98% after a few initial cycles. The in situ TEM experiments also reveal the mechanical degradation of CNFs through formation of longitudinal cracks near the c-Cld-C interface during sodiation and potassiation. Geometrical changes of the tube are explained by a chemomechanical model using the anisotropic sodiation/potassiation strains in c-C and d-C. Our results provide mechanistic insights into the electrochemical reaction, microstructure evolution and mechanical degradation of carbon-based anodes during sodiation and potassiation, shedding light onto the development of carbon-based electrodes for NIBs and KIBs.

Affiliations:

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<profileDesc><textClass><keywords scheme="KwdEn" xml:lang="en"><term>Anisotropy</term>
<term>Bilayers</term>
<term>Carbon</term>
<term>Carbon electrode</term>
<term>Electrochemical reaction</term>
<term>Interfaces</term>
<term>Microstructure</term>
<term>Nanofiber</term>
<term>Nanostructured materials</term>
<term>Sodium</term>
<term>Transmission electron microscopy</term>
</keywords>
<keywords scheme="Pascal" xml:lang="fr"><term>Microscopie électronique transmission</term>
<term>Carbone</term>
<term>Nanofibre</term>
<term>Nanomatériau</term>
<term>Bicouche</term>
<term>Sodium</term>
<term>Interface</term>
<term>Anisotropie</term>
<term>Réaction électrochimique</term>
<term>Microstructure</term>
<term>Electrode carbone</term>
<term>8107V</term>
<term>8107B</term>
<term>6865</term>
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<front><div type="abstract" xml:lang="en">Carbonaceous materials have great potential for applications as anodes of alkali-metal ion batteries, such as Na-ion batteries and K-ion batteries (NIB and KIBs). We conduct an in situ study of the electrochemically driven sodiation and potassiation of individual carbon nanofibers (CNFs) by transmission electron microscopy (TEM). The CNFs are hollow and consist of a bilayer wall with an outer layer of disordered-carbon (d-C) enclosing an inner layer of crystalline-carbon (c-C). The d-C exhibits about three times volume expansion of the c-C after full sodiation or potassiation, thus suggesting a much higher storage capacity of Na or K ions in d-C than c-C. For the bilayer CNF-based electrode, a steady sodium capacity of 245 mAh/g is measured with a Coulombic efficiency approaching 98% after a few initial cycles. The in situ TEM experiments also reveal the mechanical degradation of CNFs through formation of longitudinal cracks near the c-Cld-C interface during sodiation and potassiation. Geometrical changes of the tube are explained by a chemomechanical model using the anisotropic sodiation/potassiation strains in c-C and d-C. Our results provide mechanistic insights into the electrochemical reaction, microstructure evolution and mechanical degradation of carbon-based anodes during sodiation and potassiation, shedding light onto the development of carbon-based electrodes for NIBs and KIBs.</div>
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<name sortKey="Feifei Fan" sort="Feifei Fan" uniqKey="Feifei Fan" last="Feifei Fan">FEIFEI FAN</name>
<name sortKey="Hailong Chen" sort="Hailong Chen" uniqKey="Hailong Chen" last="Hailong Chen">HAILONG CHEN</name>
<name sortKey="Jiangwei Wang" sort="Jiangwei Wang" uniqKey="Jiangwei Wang" last="Jiangwei Wang">JIANGWEI WANG</name>
<name sortKey="Jungjohann, Katherine L" sort="Jungjohann, Katherine L" uniqKey="Jungjohann K" first="Katherine L." last="Jungjohann">Katherine L. Jungjohann</name>
<name sortKey="Ting Zhu" sort="Ting Zhu" uniqKey="Ting Zhu" last="Ting Zhu">TING ZHU</name>
<name sortKey="Yang Liu" sort="Yang Liu" uniqKey="Yang Liu" last="Yang Liu">YANG LIU</name>
<name sortKey="Yujie Zhu" sort="Yujie Zhu" uniqKey="Yujie Zhu" last="Yujie Zhu">YUJIE ZHU</name>
<name sortKey="Yunhua Xu" sort="Yunhua Xu" uniqKey="Yunhua Xu" last="Yunhua Xu">YUNHUA XU</name>
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   |texte=   In Situ Transmission Electron Microscopy Study of Electrochemical Sodiation and Potassiation of Carbon Nanofibers
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In Situ Transmission Electron Microscopy Study of Electrochemical Sodiation and Potassiation of Carbon Nanofibers

In Situ Transmission Electron Microscopy Study of Electrochemical Sodiation and Potassiation of Carbon Nanofibers

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